THERMAL SCIENCE
International Scientific Journal
FACILE PREPARATION OF α-FE2O3 NANOBULK VIA BUBBLE ELECTROSPINNING AND THERMAL TREATMENT
ABSTRACT
In this work, α-Fe2O3 nanobulk with high aspect ratio were successfully prepared via a facile bubble electrospinning technique using polyvinylidene fluoride and iron chloride hexahydrate (FeCl3•6H2O) as α-Fe2O3 precursor followed by annealing in air at 600°C. The products were characterized with field emission scanning electron microscope, Fourier transform infrared, X-ray photoelectron spectroscopy, and thermogravimetric analysis. The results showed that α-Fe2O3 nanobulk has a hierarchical heterostructure which has an extremely broad application prospect in many areas.
KEYWORDS
PAPER SUBMITTED: 2015-12-16
PAPER REVISED: 2016-02-10
PAPER ACCEPTED: 2016-02-21
PUBLISHED ONLINE: 2016-08-13
THERMAL SCIENCE YEAR
2016, VOLUME
20, ISSUE
Issue 3, PAGES [967 - 972]
- Cheng, Y. L., et al., Formation Mechanism of Fe2O3 Hollow Fibersby Direct Annealing of the Electrospun Composite Fibersand Their Mag netic, Electrochemical Properties, Cryst. Eng. Comm., 13 (2011), 8, pp. 2863-2870
- Shao, H., et al., Preparation of a-Fe2O3 Nanotubes via Electrospinning and Researchon Their Catalytic Properties, Appl. Phys. A, 108 (2012), 4, pp. 961-965
- Sundaramurthy, J., et al., Superior Photocatalytic Behaviour of Novel 1D Nanobraidand Nanoporous a-Fe2O3 Structures, RSCA Dvances, 2 (2012), 21, pp. 8201-8208
- Chris tie, T. C., et al., Electrospun a-Fe2O3 Nanorodsasa Stable, High Capacity Anode Material for Li-ion Batteries, J. Mater. Chem., 22 (2012), 24, pp. 12198-12204
- Yan, S., et al., A Novel Structure for Enhancing the Sensitivity of Gas Sensors-a-Fe2O3 Nanoropes Containinga Large Amount of Grain Boundaries and their Excellent Ethanol Sensing Performance, J. Mater. Chem. A, 3 (2015), 11, pp. 5982-5990
- Dhal, J. P., et al., Synthesis, Characterization and Photocatalytic Application of Ultra-Fine a-Fe2O3 Nanofiber, Asain Journal of Chemistry, 25 (2013), June, pp. S22-S26
- Chaudhari, S., et al., 1D Hol low a-Fe2O3 Electrospun Nanofibersas High Performance Anode Material for Lithium Ion Batteries, J. Mater. Chem., 22 (2012), 43, pp. 23049-23056
- Gao, Q., et al., Novel Hollow a-Fe2O3 Nanofibers via Electrospinning for Dye Adsorption, Nanoscale Research Letters, 10 (2015), Dec., pp. 176-183
- Nazari, M., et al., Synthesisand Characterization of Maghemite Nanopowders by Chemical Precipitation Method, J. Nanostruct. Chem., 4 (2014), June, pp.99-103
- Hua, J., et al., Hydrothermal Synthesisand Characterization of Monodisperse a-Fe2O3 Nanoparticles, Materials Letters, 63 (2009), 30, pp. 2725-2727
- Chen, R. X., et al., Bubble Rupturein Bubble Electrospinning, Thermal Science, 19 (2015), 4, pp. 1141-1149
- Dou, H., et al., A Belt-Like Super fine Film Fabricationby the Bubble-Electrospinning, Thermal Science, 17 (2013), 5, pp. 1508-1510
- Shen, J., et al., Effect of Pore Size on Gas Resistance of Nanofiber Membrane by the Bubble Electrospinning, Thermal Science, 19 (2015), 4, pp. 1349-1351
- He, J.-H., An Alternative Approach to Establishment of a Variational Principle for the Torsional Problem of Piezoelastic Beams, Applied Mathematics Letters, 52 (2016), Complete, pp. 1-3
- Chen, R. X., et al., Series Solution of the Autocatalytic Hydrolysis of Cellulose, Cellulose, 18 (2015), 5, pp. 3099-3104
- He, C. H., et al., Bubbfil Spinning for Fabrication of PVA Nanofibers, Thermal Science, 19 (2015), 2, pp. 743-746
- Liu, Z., et al., Tunable Surface Morphology of Electrospun PMMA Fiber Using Binary Solvent, Applied Surface Science, 364 (2016), Feb., pp. 516-521
- Liu, H. Y., et al., A Novel Method for Fabrication of Fascinated Nanofiber Yarns, Thermal Science, 19 (2015), 4, pp. 1331-1335
- Liu, Z,. et al., Ac tive Generation of Multiple Jets for Production Nanofiber swith High Quality and High Throughput, Material & Design, 94 (2016), Mar., pp. 496-501
- Wang, Z. Y., et al., Preparation and Catalytic Property of PVDF Composite Membrane with Polymeric Spheres Decorated by Pd Nanoparticles in Membrane Pores, Journal of Membrane Science, 496 (2015), Dec., pp. 95-107